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dc.contributor.authorRivera Guerrero, Manuel Andres.-
dc.date.accessioned2022-06-23T03:05:07Z-
dc.date.available2017-03-15-
dc.date.available2022-06-23T03:05:07Z-
dc.date.issued2017-
dc.identifier.citationRivera Guerrero, M. A. (2016). Caracterización de la materia de construcción (Batumen), de los nidos de cuatro especies de abejas sin aguijón presentes en Norte de Santander (Colombia) [Trabajo de Grado Pregrado, Universidad de Pamplona]. Repositorio Hulago Universidad de Pamplona. http://repositoriodspace.unipamplona.edu.co/jspui/handle/20.500.12744/2261es_CO
dc.identifier.urihttp://repositoriodspace.unipamplona.edu.co/jspui/handle/20.500.12744/2261-
dc.descriptionEn el presente trabajo se realizó la caracterización del batumen (material de construcción) proveniente de nidos de cuatro especies de abejas sin aguijón: Melipona favosa favosa, Melipona compressipes, Melipona fuscipes y Partamona sp., ubicados en los municipios de los Patios y Pamplonita del departamento Norte de Santander, utilizando diversas técnicas analíticas como: espectrometría infrarroja (FTIR-ATR), análisis termogravimétrico (TGA) simultáneo con calorimetría diferencial de barrido (DSC), Difracción de rayos X (DRX) y Fluorescencia de rayos X (FRX). El análisis termogravimétrico (TGA) permitió determinar que la pérdida de peso para todas la muestras debido a la humedad fue de 2-4%, y la pérdida de peso no asociada a la humedad varió de 1,30% a 10,95%. Con la calorimetría diferencial de barrido (DSC) se encontró en todas la muestras la presencia de dos picos, el primero se encontró en un rango de temperatura de 39,41 o C a 196,54 o C con una variación de entalpía de 220,13 (J/g) a 396,6 (J/g). El segundo se encontró en un rango de temperatura de 195,78 o C a 804,22 o C con una variación de entalpía de 13272 (J/g) a 24613,66 (J/g). La técnica de difracción de rayos X (FRX) permitió determinar la composición elemental de las muestras que mayoritariamente contienen SiO2 (60,94% -66,83%), Al2O3 (15,85% - 21,25%) y Fe2O3 (7,16% - 8,90%). Los resultados de la espectroscopía infrarroja (FTIR-ATR) confirmaron la presencia de compuestos inorgánicos como SiO2, Fe2O3, entre otros, y de compuestos orgánicos como alcanos, alquenos, alcoholes, esteres, halogenuros ácidos, amidas secundarias y compuestos halogenados. La cristalinidad de las muestras, se determinó mediante difracción de rayos X (DRX), observando mediante esta técnica que los minerales cuarzo y moscovita están presentes en el batumen de las diferentes especies.es_CO
dc.description.abstractThis work shows a characterization of the batumen (building material used by bees) from nests of four species of stingless bees: Melipona favosa favosa, Melipona compressipes, Melipona fuscipes and Partamona sp., located in the municipalities of Los Patios and Pamplonita (Norte de Santander), using analytical techniques such as: infrared spectroscopy (FTIR-ATR), simultaneous thermogravimetric analysis (TGA) / differential scanning calorimetry (DSC), X-ray diffraction (XRD) and X-ray fluorescence (FRX). Thermogravimetric analysis (TGA) allowed determining weight loss on samples. The percentage of moisture in all samples was ranging between 2 to 4%, and weight loss not associated with moisture ranged from 1.30% to 10.95%. With the technique differential scanning calorimetry (DSC) the presence of two peaks was found in all samples, the first one was found in a temperature range of 39.41 o C to 196.54 o C with an enthalpy variation of 220.13 ( J / g) at 396.6 (J / g). The second one was found in a temperature range of 195.78 o C to 804.22 o C with a change in enthalpy of 13272 (J / g) to 24613.66 (J / g). The X-ray diffraction (FRX) permitted the determination of the elemental composition. All samples have SiO2 (60.94% - 66.83%), Al2O3 (15.85% - 21.25%) and Fe2O3, 16% - 8.90%). The results of infrared spectroscopy (FTIR-ATR) confirmed the presence of inorganic compounds such as SiO2, Fe2O3, among others, and organic compounds such as alkanes, alkenes, alcohols, esters, acid halides, secondary amides and halogen compounds. The crystallinity was determined by X-ray diffraction (XRD). This technique showed that Quartz and muscovite were found in the batumen samples.es_CO
dc.format.extent61es_CO
dc.format.mimetypeapplication/pdfes_CO
dc.publisherUniversidad de Pamplona – Facultad de Ingenierías y Arquitectura.es_CO
dc.subjectEl autor no proporciona la información sobre este ítem.es_CO
dc.titleCaracterización de la materia de construcción (Batumen), de los nidos de cuatro especies de abejas sin aguijón presentes en Norte de Santander, (Colombia).es_CO
dc.typehttp://purl.org/coar/resource_type/c_7a1fes_CO
dc.date.accepted2016-12-15-
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